反应详情

Prepared from 3-benzyloxycarbonylamino-3-methyl-N-[2,3,4,5-tetrahydro-2-oxo-1H-1-benzazepin-3-yl]-butanamide (Example 51, Step A) and 3-phenylpropyl bromide by the procedure described in Example 3, Step A. 1H NMR (200 MHz, CDCl3): 1.38 (s,6H), 1.82 (m,4H), 2.4-2.9 (m,7H), 3.45 (m,1H), 4.36 (m,1H), 5.02 (s,2H), 5.64 (s,1H), 6.69 (d,8 Hz,1H), 6.9-7.4 (m,14H). FAB-MS: calculated for C32H37N3O4 527; found 528 (M+H,100%).