HRID1643595

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：COC(=O)c1cc(Oc2ccc(S(C)(=O)=O)cc2Cl)c2c(c1)OC(C)(C)C2

HCID59560316

未命名化合物

结构：CC1(C)Cc2c(Oc3ccc(S(C)(=O)=O)cc3)cc(C(=O)O)cc2O1

HCID59560427

未命名化合物

PRODUCTS

生成物

结构：CC1(C)Cc2c(Oc3ccc(S(C)(=O)=O)cc3Cl)cc(C(=O)O)cc2O1

HCID59560228

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in a similar manner as described for Intermediate 15a, from 4-(2-chloro-4-methanesulfonyl-phenoxy)-2,2-dimethyl-2,3-dihydro-benzofuran-6-carboxylic acid methyl ester (119a). 1H NMR (400 MHz, CDCl3) δ 8.08 (d, J=2.27 Hz, 1 H) 7.78 (dd, J=8.59, 2.27 Hz, 1 H) 7.34 (d, J=1.26 Hz, 1 H) 7.23 (d, J=1.26 Hz, 1 H) 7.00 (d, J=8.59 Hz, 1 H) 3.11 (s, 3 H) 2.95 (s, 2 H) 1.52 (s, 6 H); LCMS for C18H17ClO6S m/z 397.00 (M+H)+.