HRID1662200

反应详情

EQUATION

反应方程式

REACTANTS

反应物

$结构：CC(C)(C)S(=O)/N=C(\c1cccc(Br)c1)c1cccc(F)c1C#N$

HCID58579486

未命名化合物

结构：COc1c(C)cc(Br)cc1CO[Si](C)(C)C(C)(C)C

HCID67417833

未命名化合物

PRODUCTS

生成物

结构：COc1c(C)cc(C2(c3cccc(Br)c3)N=C(N)c3c(F)cccc32)cc1CO

HCID58579488

未命名化合物

收率 54%

PROCEDURE

实验过程

The title compound was synthesized as described for Example 35i in 54% yield, starting from of (5-bromo-2-methoxy-3-methylbenzyloxy)(tert-butyl)dimethylsilane (1.44 g, 4.17 mmol) and (E)-N-((3-bromophenyl)(2-cyano-3-fluorophenyl)methylene)-2-methylpropane-2-sulfinamide (1.415 g, 3.47 mmol). MS (ES+) m/z 455, 457 [M+H]+.