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HRID1824234

反应详情

EQUATION

反应方程式

HRID 1824234 的结构方程式

REACTANTS

反应物

3
结构：CCC(NC(=O)OC(C)(C)C)C(=O)O
HCID333522

2-[(tert-Butoxycarbonyl)amino]butanoic acid

C9H17NO4

结构：CCC(N)C(=O)OC.Cl
HCID13283515

Methyl 2-aminobutanoate--hydrogen chloride (1/1)

C5H12ClNO2

结构：COC(=O)C(NC(=O)[C@H](C)NC(=O)OC(C)(C)C)C1CC1
HCID58583288

未命名化合物

PRODUCTS

生成物

1
结构：CCC(NC(=O)OC(C)(C)C)C(=O)N[C@@H](C)C(=O)OC
HCID86588879

未命名化合物

PROCEDURE

实验过程

Following the procedure for the preparation of methyl{[N-(tert-butoxycarbonyl)-L-alanyl]amino}(cyclopropyl)acetate but substituting N-Boc-alpha-aminobutyric acid and methyl 2-aminobutanoate hydrochloride and making non-critical variations provided the title compound as a solid: 1H NMR (CDCl3) δ 0.82–0.91, 1.24–1.38, 1.52, 1.68–2.05, 3.75, 4.20, 4.52–4.59, 5.05, 6.69.