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HRID1887178

反应详情

EQUATION

反应方程式

HRID 1887178 的结构方程式

REACTANTS

反应物

2
结构：C1CCN(C2CCNCC2)CC1
HCID78607

1,4′-Bipiperidine

C10H20N2

结构：Clc1ccc(-c2cccnc2)nn1
HCID16732435

3-Chloro-6-(pyridin-3-yl)pyridazine

C9H6ClN3

PRODUCTS

生成物

1
结构：c1cncc(-c2ccc(N3CCC(N4CCCCC4)CC3)nn2)c1
HCID58006568

1'-[6-(Pyridin-3-yl)pyridazin-3-yl]-1,4'-bipiperidine

C19H25N5

PROCEDURE

实验过程

The title compound was prepared by a similar procedure to that described in Example 1, starting from 3-chloro-6-(pyridin-3-yl)-pyridazine and 4-piperidinopiperidine. 1H NMR (400 MHz, CD3OD) δ 9.47 (d, 1H), 9.11 (dt, 1H), 8.93 (d, 1H), 8.40 (d, 1H), 8.15 (q, 1H), 7.94 (d, 1H), 4.66 (d, 2H), 3.66 (m, 1H), 3.58 (d, 2H), 3.36 (t, 2H), 3.08 (t, 2H), 2.38 (d, 2H), 1.80-2.00 (m, 7H), 1.54 (m, 1H).