HRID1887834

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID506057

4-Carbamoylbenzoic acid

C8H7NO3

结构：NCc1c(-c2ncco2)n(-c2ccccc2)c2cc(Cl)ccc2c1=O

HCID71208332

未命名化合物

PRODUCTS

生成物

结构：NC(=O)c1ccc(C(=O)NCc2c(-c3ncco3)n(-c3ccccc3)c3cc(Cl)ccc3c2=O)cc1

HCID71208768

未命名化合物

PROCEDURE

实验过程

N-(7-Chloro-2-oxazol-2-yl-4-oxo-1-phenyl-1,4-dihydro-quinolin-3-ylmethyl)-terephthal-amide was prepared starting from intermediate A and 4-(aminocarbonyl)benzoic acid. 1H NMR (400 MHz, DMSO-d6) δ ppm 8.40 (t, J=4.50 Hz, 1H) 8.31 (d, J=8.59 Hz, 1H) 8.02 (br. s, 1H) 7.97 (d, J=0.78 Hz, 1H) 7.83-7.87 (m, 2H) 7.73-7.78 (m, 2H) 7.37-7.54 (m, 7H) 7.16 (d, J=0.78 Hz, 1H) 6.72 (d, J=1.56 Hz, 1H) 4.25 (d, J=4.30 Hz, 2H). MS calcd. for C27H19ClN4O4 [(M+H)+] 499.1, obsd. 499.