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HRID1911071

反应详情

EQUATION

反应方程式

HRID 1911071 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)O[C@H]2CCN(C(=O)OC(C)(C)C)C2)cc1
HCID57957824

tert-Butyl (3S)-3-[(4-methylbenzene-1-sulfonyl)oxy]pyrrolidine-1-carboxylate

C16H23NO5S

结构：C[C@@H]1CCCN1[C@H]1CCN(C(=O)OC(C)(C)C)C1
HCID59401895

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CCCN1[C@@H]1CCN(C(=O)OC(C)(C)C)C1
HCID59401893

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in a manner substantially the same as intermediate (2R,3′S)-2-Methyl-[1,3′]bipyrrolidinyl-1′-carboxylic acid tert-butyl ester by condensing 3-(3S)-(toluene-4-sulfonyloxy)-pyrrolidine-1-carboxylic acid tert-butyl ester and R-(−)-2-methylpiperindine (obtained from Advanced Asymmetrics). LCMS: RT=1.09 minutes, MS: 255 (M+H).