反应详情

The title compound was synthesized using (Z)-4-(4-(4-aminophenylthio)quinolin-2(1H)-ylidene)-3-propyl-1H-pyrazol-5(4H)-one and 3-(diethylamino)propanoyl chloride in THF according to the procedure described in the synthesis of Example 26. 1H NMR (400 MHz, DMSO-d6) δ ppm 0.71 (t, J=7.45 Hz, 3H) 1.23 (t, J=7.20 Hz, 6H) 1.28-1.37 (m, 2H) 2.19-2.29 (m, 2H) 2.88 (t, J=7.07 Hz, 2H) 3.18 (ddd, J=12.69, 6.82, 6.51 Hz, 4H) 3.38-3.42 (m, 2H) 6.78 (s, 1H) 7.54-7.62 (m, 1H) 7.71 (d, J=8.59 Hz, 2H) 7.79-7.90 (m, 4H) 8.09 (d, J=8.34 Hz, 1H) 9.12 (s, 1H) 10.57 (s, 1H); ESI-MS: m/z calc'd for C28H33N5O2S 503.66. found 504.2 (M+H)+.

1. customdescribed in the synthesis of Example 26