反应详情

The title compound was prepared from (Z)-4-(4-chloroquinolin-2(1H)-ylidene)-3-cyclohexyl-1H-pyrazol-5(4H)-one and 4-aminothiophenol using the procedure described in Example 48. 1H NMR (400 MHz, DMSO-d6) δ ppm 1.08-1.19 (m, 3H) 1.29-1.40 (m, 2H) 1.58-1.65 (m, 4H) 1.67 (d, J=9.60 Hz, 2H) 2.37 (t, J=10.23 Hz, 1H) 6.76 (d, J=8.59 Hz, 2H) 6.90 (s, 1H) 7.33 (d, J=8.34 Hz, 2H) 7.63 (t, J=7.33 Hz, 1H) 7.85-7.93 (m, 2H) 8.16 (d, J=8.34 Hz, 1H); ESI-MS: m/z calc'd for C24H24N4OS 416.54. found m/z 417.1 (M+H)+.