反应详情

The title compound was prepared from (Z)-3-benzyl-4-(4-chloroquinolin-2(1H)-ylidene)-1H-pyrazol-5(4H)-one and 4-aminothiophenol under conditions similar to those described in Example 6. 1H NMR (400 MHz, DMSO-d6) δ ppm 2.81 (s, 2H) 6.77-6.79 (m, 3H) 7.23-7.30 (m, 3H) 7.33 (d, J=8.34 Hz, 2H) 7.40-7.48 (m, 2H) 7.64 (t, J=7.45 Hz, 1H) 7.88 (t, J=7.83 Hz, 1H) 7.96 (d, J=8.59 Hz, 1H) 8.14 (d, J=8.08 Hz, 1H); ESI-MS: m/z calc'd for C25H20N4OS 424.14. found 424.2 (M+H)+.