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HRID20707

反应详情

EQUATION

反应方程式

HRID 20707 的结构方程式

REACTANTS

反应物

2
结构：C[Si](C)(C)ON
HCID2734666

O-(Trimethylsilyl)hydroxylamine

C3H11NOSi

结构：COc1ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc2c1OCC(=O)O
HCID24849714

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc2c(Nc3c(Cl)cncc3Cl)cc(=O)oc2c1OCC(=O)NO
HCID24849298

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 2-(4-(3,5-dichloropyridin-4-ylamino)-7-methoxy-2-oxo-2H-chromen-8-yloxy)acetic acid (Example 49) following the procedure outlined in Example 84 (except TMSONH2 in place of NH2OH•HCl). 1H NMR (400 MHz, DMSO-d6): δ 10.64 (s, 1H), 9.54 (s, 1H), 8.82 (s, 2H), 7.97 (d, 1H), 7.23 (d, 1H), 4.65 (s, 1H), 4.43 (s, 2H), 3.93 (s, 3H); MS (ESI): 425.8.