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HRID23297

反应详情

EQUATION

反应方程式

HRID 23297 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ncc(Cl)cc1Br
HCID22591246

3-Bromo-5-chloropyridine-2-carbonitrile

C6H2BrClN2

结构：CC(C)(C)OC(=O)N1CC[C@H]2[C@@H](C1)c1cc(N)cc3c1N2CCOC3
HCID86586438

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Cl.N#Cc1ncc(Cl)cc1Nc1cc2c3c(c1)[C@@H]1CNCC[C@@H]1N3CCOC2
HCID131724730

未命名化合物

PROCEDURE

实验过程

Following the procedures described in Example 176 and using 3-bromo-5-chloro-2-cyanopyridine, tert-butyl (7bR,11aS)6-amino-1,2,7b,10,11,11a-hexahydro-4H-[1,4]oxazepino[6,5,4-hi]pyrido[4,3-b]indole-9(8H)-carboxylate from Example 56, Part B was converted into the title compound of Example 177. ESI MS m/z 382.3/384.3 [C20H20CIN5O+H]+.