HRID248940

反应详情

EQUATION

反应方程式

HRID 248940 的结构方程式

PROCEDURE

实验过程

Preparation is effected analogously to Example 1, using 0.7 g (2.3 mmol) of N-methyl-N-[3-phenyl-3-(2-pyridyl)propyl]-1,4-butanediamine and 0.89 g (2.3 mmol) of N-cyano-O-phenyl-N'-[3-[3-(piperidinomethyl)phenoxy]propyl]isourea as starting materials. Working up by chromatography analogously to Example 1 yields the purified title compound in the form of a viscous oil; MS (+FAB method): m/z (rel. int.[%])=596 ([M+H]+ 7), 196 (100).

WORKUP

后处理

  1. customPreparation
  2. customWorking up by chromatography analogously to Example 1 yields the
  3. custompurified title compound in the form of a viscous oil