HRID253405

反应详情

EQUATION

反应方程式

HRID 253405 的结构方程式

PROCEDURE

实验过程

were prepared following the protocol of Scheme 20, substituting iodoethane with iodomethane in Step 3 to provide P-1891, or substituting iodoethane with 2-iodo-1,1,1-trifluoroethane in Step 3 to provide P-2076, or substituting iodoethane with 2-iodo-1-fluoroethane in Step 3 to provide P-2118, or substituting 4-chlorobenzyl bromide 22 with 4-chloro-2-fluoro-benzyl bromide in Step 1 and 7-azaindole 6 with 5-methoxy-7-azaindole in Step 4 to provide P-2016. MS (ESI) [M+H+]+=393.4 (P-1891), 461.08 (P-2076), 455.2 (P-2016), and 425.17 (P-2118).

WORKUP

后处理

  1. customto provide P-2076
  2. customto provide P-2118
  3. customto provide P-2016