HRID280306

反应详情

EQUATION

反应方程式

HRID 280306 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in the manner described in Example 3, replacing 2-(3-chlorophenyl)-2-hydroxy ethanamine by 2-(3-trifluoromethylphenyl)-2-hydroxyethanamine, and 4-methylphenylacetone by 4-(4-methylphenyl)butan-2-one. The chromatographed material was recrystallised from hexane to give the title compound mp 52°-55° as a 44:56 ratio of diastereoisomers.

WORKUP

后处理

  1. customThe title compound was prepared in the manner
  2. customThe chromatographed material was recrystallised from hexane