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HRID29187

反应详情

EQUATION

反应方程式

HRID 29187 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：O=C(N[C@@H](Cc1ccccc1)[C@H](O)CN(OC1CCCC1)S(=O)(=O)c1ccc(OCCN2CCOCC2)cc1)O[C@H]1CO[C@H]2OCC[C@H]21
HCID21356324

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N[C@@H](Cc1ccccc1)[C@H](O)CN(OC1CCCC1)S(=O)(=O)c1cccc(OCCN2CCOCC2)c1)O[C@H]1CO[C@H]2OCC[C@H]21
HCID86585038

未命名化合物

PROCEDURE

实验过程

This compound was prepared from Example 44 under the same conditions used for the preparation of Example 98 (3R,3aS,6aR)hexahydrofuro[2,3-b]furan-3-yl N-[(1S,2R)-1-benzyl-3-((cyclopentyloxy)[4-(2-morpholinoethoxy)phenyl]sulfonylamino)-2-hydroxypropyl]carbamate. Rf=0.15 (ethyl acetate); H1-NMR (CDCl3): δ 7.44-7.14 (10H,m), 5.62 (1H,s), 5.00 (1H,m), 4.79 (2H,m), 4.16 (2H,m), 3.98-3.60 (10H,m), 3.12 (1H,bs), 3.02-2.71 (8H,m), 2.58 (4H,m), 1.90-1.72 (4H,m), 1.72-1.42 (4H, m); MS (ESI): M+H=690.

WORKUP

后处理

  1. customThis compound was prepared from Example 44 under the same conditions