HRID444421

反应详情

EQUATION

反应方程式

HRID 444421 的结构方程式

PROCEDURE

实验过程

The following analysis compares a typical APAP product produced by the stepwise/boric acid process of this invention with high purity standards. For this example 30 lbs. of p-nitrophenol was hydrogenated at 63°-67° C. by stepwise acetylation using 10 mole percent boric acid and adding 50% acetic anhydride after completing 60% of the hydrogenation. Product yield was about 85%.

WORKUP

后处理

  1. customwas hydrogenated at 63°-67° C. by stepwise acetylation