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HRID50931

反应详情

EQUATION

反应方程式

HRID 50931 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(OC(F)(F)F)cc1[N+](=O)[O-]
HCID2775772

2-Nitro-4-(trifluoromethoxy)aniline

C7H5F3N2O3

结构：FC(F)(F)c1ccc2c(c1)nc(/C=C/c1ccccc1)n2-c1ccccn1
HCID22736704

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)(F)Oc1ccc2c(c1)nc(/C=C/c1ccccc1)n2-c1ccccn1
HCID22736725

未命名化合物

PROCEDURE

实验过程

The titled compound was prepared from 2-nitro4-trifluoromethoxyaniline according to the preparation of (E)-1-(2-pyridyl)-2-styryl-5-trifluoromethyl-1H-benzimidazole (Example 57). MW: 381.36; mp: 92.0-93.0° C.; 1H-NMR (CDCl3) δ: 8.81-8.77 (1H, m), 8.02 (1H, d, J=16.5 Hz), 8.05-7.98 (1H, m), 7.71-7.68 (1H, m), 7.54-7.45 (4H, m), 7.45 (1H, d, J=8.8 Hz), 7.42-7.30 (3H, m), 7.17-7.10 (1H, m), 7.10 (1H, d, J=16.1 Hz)