HRID511036

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC1(C)OB(c2cncc(S(C)(=O)=O)c2)OC1(C)C

HCID53398530

3-(Methanesulfonyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

C12H18BNO4S

HCID86666857

未命名化合物

PRODUCTS

生成物

结构：CC(=O)c1cc(Cl)c(F)c(-c2cncc(S(C)(=O)=O)c2)c1O

HCID86666957

未命名化合物

收率 87%

PROCEDURE

实验过程

The desired compound was prepared according to the procedure of Example 127, step A, using 1-(5-chloro-4-fluoro-2-hydroxy-3-iodophenyl)ethanone (See, Example 172, Step 2) and 3-(methylsulfonyl)-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine (PepTech Corp., Cat. No. BE358) as the starting materials in 87% yield. LCMS for C14H12ClFNO4S (M+H)+: m/z=344.0. Found: 343.9.