huagongshe.com
HRID525479

反应详情

EQUATION

反应方程式

HRID 525479 的结构方程式

REACTANTS

反应物

2
结构：CCOC(=O)C1CCN(Cc2ccc3cc(O[C@@H]4C[C@H](CC)CC[C@H]4C(C)C)ccc3c2)CC1
HCID117736827

未命名化合物

结构：CCOC(=O)C1CCN(Cc2ccc3cc(O[C@H]4CC[C@@H](c5ccccc5)CC4)ccc3c2)CC1
HCID178469205

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C1CCN(Cc2ccc3cc(O[C@@H]4C[C@H](C)CC[C@H]4C(C)C)ccc3c2)CC1
HCID68352983

未命名化合物

收率 38%

PROCEDURE

实验过程

The preparation of ethyl 1-((6-(((1R,2S,5R)-2-isopropyl-5-ethylcyclohexyl)oxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate was the same as that of ethyl 1-((6-((cis-4-phenylcyclohexyl)oxy)naphthalen-2-yl)methyl)piperidine-4-carboxylate. 82 mg, slight yellow oil, yield: 38%. ESI-MS (M+1)+: 452.2. 1H NMR (400 MHz, CDCl3) δ: 7.66-7.63 (m, 3H), 7.40-7.39 (m, 1H), 7.08-7.05 (m, 2H), 4.12-4.03 (m, 3H), 3.54 (s, 2H), 2.84-2.80 (m, 1H), 2.25-2.15 (m, 2H), 1.81-1.69 (m, 1H), 1.70-1.66 (m, 2H), 1.25-1.15 (m, 11H), 1.10-0.91 (m, 4H), 0.87 (d, J=6.8 Hz, 6H), 0.71 (d, J=6.8 Hz, 3H).