huagongshe.com
HRID529584

反应详情

EQUATION

反应方程式

HRID 529584 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)[C@H](CC[C@H](Cc1ccccc1)C(=O)O)Cc1ccccc1
HCID68292409

未命名化合物

结构：CCCNC(=O)[C@@H]1CCC[C@@H]2SCC[C@H](N)C(=O)N21.Cl
HCID68292610

未命名化合物

PRODUCTS

生成物

1
结构：CCCNC(=O)[C@@H]1CCC[C@@H]2SCC[C@H](NC(=O)[C@H](CC[C@H](Cc3ccccc3)C(=O)N[C@H]3CCS[C@H]4CCC[C@@H](C(=O)NCCC)N4C3=O)Cc3ccccc3)C(=O)N21
HCID86706245

未命名化合物

PROCEDURE

实验过程

(2R,5R)-2,5-Dibenzyl-N1,N6-bis((4S,7S,10aS)-5-oxo-7-(propylcarbamoyl)octahydro-2H-pyrido[2,1-b][1,3]thiazepin-4-yl)hexanediamide was synthesized as described in General Procedure F using Intermediate 3 (7.9 mg, 0.024 mmol) and Intermediate 38 (18 mg, 0.056 mmol) to give a light yellow solid (15 mg, 70% yield). Anal. Calcd. for C46H64N6O6S2 m/z 860.7. found: 861.6 (M+H)+; 1H NMR (400 MHz, CDCl3) δ ppm 7.24-7.13 (m, 10H), 5.31 (m, 2H), 4.94 (m, 4H), 3.33-3.13 (m, 6H), 2.76 (m, 6H), 2.35 (m, 4H), 2.08 (m, 4H), 1.70-1.47 (m, 18H), 0.90 (m, 6H).