HRID555908

反应详情

EQUATION

反应方程式

HRID 555908 的结构方程式

PROCEDURE

实验过程

The title compound was prepared essentially according to the method of Example 4, but using 5-Chloro-2-(1H-tetrazol-5-yl)aniline (1.0 mmol) and 3-methoxybenzoyl chloride to afford the desired product (29.1 mg, 9%). 1H NMR (400 MHz, d6-DMSO): δ 10.81 (s, 1H), 8.75 (s, 1H), 8.06 (s, 1H), 7.60 (m, 3H), 7.25 (s, 1H), 3.89 (s, 3H). MS (EI) for C15H12ClN5O2: 329.7 (M+H).

WORKUP

后处理

  1. customThe title compound was prepared essentially