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HRID56568

反应详情

EQUATION

反应方程式

HRID 56568 的结构方程式

REACTANTS

反应物

2
结构：COc1cc(-c2ccco2)cc(OC)c1Br
HCID58431988

未命名化合物

结构：COC(C(=O)N(C)OC)c1ccc(CN(C)C)cc1
HCID58432061

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc(-c2ccc(C(=O)C(OC)c3ccc(CN(C)C)cc3)o2)cc(OC)c1Br
HCID58432105

未命名化合物

PROCEDURE

实验过程

1-(5-(4-Bromo-3,5-dimethoxyphenyl)furan-2-yl)-2-(4-((dimethylamino)methyl)phenyl)-2-methoxyethanone was prepared from 2-(4-bromo-3,5-dimethoxyphenyl)furan and 2-(4-((dimethylamino)methyl)phenyl)-N,2-dimethoxy-N-methylacetamide according to the procedure used in Example 30. Purification by chromatography (4% MeOH/CH2Cl2) gave the product as a pale yellow oil (0.004 g, 1% yield). MS: ink 488.3 [M+H]+.

WORKUP

后处理

  1. customPurification by chromatography (4% MeOH/CH2Cl2)