huagongshe.com
HRID599488

反应详情

EQUATION

反应方程式

HRID 599488 的结构方程式

REACTANTS

反应物

2
结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

结构：CCOC(=O)c1csc(S(=O)(=O)N2CCC(Sc3cc(C(C)(C)C)c(O)c(C(C)(C)C)c3)CC2)n1
HCID86635437

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(SC2CCN(S(=O)(=O)c3nc(CO)cs3)CC2)cc(C(C)(C)C)c1O
HCID25168151

未命名化合物

PROCEDURE

实验过程

The title compound was prepared (116 mg, clear oil) in a manner similar to Ex. 5 from ethyl 2-[4-(3,5-di-tert-butyl-4-hydroxy-phenylsulfanyl)-piperidine-1-sulfonyl]-thiazole-4-carboxylate (Ex. 19e) and LiAlH4. 1H-NMR (400 MHz, CDCl3): δ 7.51 (s, 1H), 7.23 (s, 2H), 5.31 (s, 1H), 4.84 (s, 2H), 3.80 (m, 2H), 2.90 (m, 2H), 2.42 (bs, 1H), 1.99 (m, 2H), 1.68 (m, 2H), 1.39 (s, 18H).