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HRID656565

反应详情

EQUATION

反应方程式

HRID 656565 的结构方程式

REACTANTS

反应物

2
结构：COCCON1C(=O)c2ccccc2C1=O
HCID12919115

2-(2-Methoxyethoxy)-1H-isoindole-1,3(2H)-dione

C11H11NO4

结构：CC(C)(C)OC(=O)NCCON1C(=O)c2ccccc2C1=O
HCID18929164

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)NCCON
HCID15610443

1,1-Dimethylethyl N-[2-(aminooxy)ethyl]carbamate

C7H16N2O3

收率 58%

PROCEDURE

实验过程

2E was deprotected as previously described in 2A, Step 2 to give tert-butyl 2-(aminooxy)ethylcarbamate (2F, 1.26 g, 58% yield). 1H NMR (400 MHz, CHLOROFORM-d) δ ppm 1.45 (s, 9H) 3.37 (q, J=5.31 Hz, 2H) 3.62-3.85 (m, 2H) 4.90 (br. s., 1H) 5.47 (br. s., 2H).