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HRID710362

反应详情

EQUATION

反应方程式

HRID 710362 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc2c(C(=O)c3cc(OC)c(OC)c(OC)c3)cn(S(=O)(=O)c3ccc(CCC4(NC(=O)OC(C)(C)C)COC(C)(C)OC4)cc3)c2c1
HCID131733939

未命名化合物

结构：CC(C)Oc1ccc(CCC2(NC(=O)OC(C)(C)C)COC(C)(C)OC2)cc1C12CC3CC(CC(C3)C1)C2
HCID131733956

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(CCC(N)(CO)CO)cc1C12CC3CC(CC(C3)C1)C2
HCID46195172

未命名化合物

收率 67%

PROCEDURE

实验过程

When the product of Step C was substituted for tert-butyl-5-(4-(6-methoxy-3-(3,4,5-trimethoxybenzoyl)-1H-indol-1-ylsulfonyl)-phenethyl)-2,2-dimethyl-1,3-dioxan-5-ylcarbamate in Example 13, Step F, the similar process afforded the title compound in 67% yield, as a creamy paste. 1H-NMR (CDCl3) 1.28 (d, 6H, J=6 Hz); 1.68 (s, 6H); 1.82-1.88 (m, 2H); 1.97 (s, 3H); 2.02 (s, 6H); 2.47-2.54 (m, 2H); 3.61 (d, 2H, J=12.1 Hz); 3.68 (d, 2H, J=12.1 Hz); 4.48-4.57 (m, 1H); 6.68 (d, 1H, J=8.4 Hz); 6.88 (dd, 1H, J=8.29, 2.1 Hz); 6.94 (d, 1H, J=2.14 Hz).