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HRID724614

反应详情

EQUATION

反应方程式

HRID 724614 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)[Si](C)(C)Oc1cccc(B(O)O)c1
HCID3463029

(3-{[tert-Butyl(dimethyl)silyl]oxy}phenyl)boronic acid

C12H21BO3Si

结构：CC(C)(C)N1C(=O)C=C(Cl)S1(=O)=O
HCID21878638

2-tert-Butyl-5-chloro-1H-1lambda~6~,2-thiazole-1,1,3(2H)-trione

C7H10ClNO3S

PRODUCTS

生成物

1
结构：CC(C)(C)N1C(=O)C=C(c2cccc(O[Si](C)(C)C(C)(C)C)c2)S1(=O)=O
HCID58746859

未命名化合物

PROCEDURE

实验过程

This compound was prepared according to the procedure of Example 1.1, Step 4, using 9-A and 3-(t-butyldimethylsilyoxy)phenylboronic acid as the starting materials. 1H NMR (500 MHz, CDCl3): δ 7.37–7.36 (m, 2H), 7.25–7.24 (m, 1H), 7.03–7.01 (m, 1H), 6.61 (s, 1H), 1.73 (s, 9H), 0.99 (s, 9H), 0.23 (s, 6H); LCMS found for C19H29NO4SSi (M+H)+: m/z=418.

WORKUP

后处理

  1. customThis compound was prepared