HRID749479

反应详情

EQUATION

反应方程式

HRID 749479 的结构方程式

PROCEDURE

实验过程

The compound was synthesized in an analogous way to that of Method 21b but using 6-cyano-N-[(2S)-2-(4-fluorophenyl)pent-4-en-1-yl]-N-methylindane-4-carboxamide rather than 3,5-dichloro-N-[(2S)-2-(4-fluorophenyl)pent-4-en-1-yl]-N-methylbenzamide (yield, 89%). 1H NMR (300 MHz, CDCl3): 0.9-4.2 (cm, 14H), 5.9 (s, <1H), 6.6-8.2 (cm, 6H), 8.0 (s, <1H), 9.8 (s, 1H).

WORKUP

后处理

  1. customThe compound was synthesized in an analogous way to that of Method 21b