HRID749482

反应详情

EQUATION

反应方程式

HRID 749482 的结构方程式

PROCEDURE

实验过程

The compound was synthesized in an analogous way to that of Method 20b but using 3-fluoro-N-[(2S)-2-(4-fluorophenyl)pent-4-en-1-yl]-N-methyl-5,6,7,8-tetrahydronaphthalene-1-carboxamide rather than N-[(2S)-2-(4-fluorophenyl)pent-4-en-1-yl]-N-methyl-3,5-bis(trifluoromethyl)benzamide (yield, 68%). 1H NMR (500 MHz, CDCl3): 1.6-4.2 (cm, 16H), 6.2-7.8 (cm, 6H), 9.8 (s, 1H).

WORKUP

后处理

  1. customThe compound was synthesized in an analogous way to that of Method 20b