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HRID879564

反应详情

EQUATION

反应方程式

HRID 879564 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc2nc(-c3ccc4c(C)nn(C)c4c3)sc2c(-c2ccc(Cl)cc2)c1[C@H](OC(C)(C)C)C(=O)O
HCID86700214

未命名化合物

结构：CCOC(=O)[C@@H](OC(C)(C)C)c1c(C)cc2nc(-c3ccc4nn(Cc5ccccc5)c(C)c4c3)sc2c1-c1ccc(Cl)cc1
HCID86700389

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc2nc(-c3ccc4nn(Cc5ccccc5)c(C)c4c3)sc2c(-c2ccc(Cl)cc2)c1[C@H](OC(C)(C)C)C(=O)O
HCID86700388

未命名化合物

PROCEDURE

实验过程

Prepared in a manner similar to (S)-2-tert-butoxy-2-(7-(4-chlorophenyl)-2-(1,3-dimethyl-1H-indazol-6-yl)-5-methylbenzo[d]thiazol-6-yl)acetic acid, but using (S)-ethyl 2-(2-(2-benzyl-3-methyl-2H-indazol-5-yl)-7-(4-chlorophenyl)-5-methylbenzo[d]thiazol-6-yl)-2-tert-butoxyacetate instead of (S)-ethyl 2-tert-butoxy-2-(7-(4-chlorophenyl)-2-(1,3-dimethyl-1H-indazol-6-yl)-5-methylbenzo[d]thiazol-6-yl)acetate. LCMS-ESI+: calc'd for C35H33ClN3O3S: 610.2 (M+H+); found: 610.3 (M+H+). 1H NMR (400 MHz, CD3OD) δ 8.36 (s, 1H), 7.99 (dd, J=9.1, 1.6 Hz, 1H), 7.80 (s, 1H), 7.69 (d, J=8.6 Hz, 1H), 7.65 (d, J=9.1 Hz, 1H), 7.59 (t, J=3.4 Hz, 3H), 7.38-7.26 (m, 3H), 7.17 (d, J=7.0 Hz, 2H), 5.65 (s, 2H), 5.26 (s, 1H), 2.64 (s, 3H), 2.61 (s, 3H), 0.98 (s, 9H).