huagongshe.com
HRID969610

反应详情

EQUATION

反应方程式

HRID 969610 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)n2ccc3ccccc32)cc1
HCID10956616

N-Tosylindole

C15H13NO2S

结构：COC1(OC)C=CC(=O)c2ccccc21
HCID11095717

4,4-dimethoxy-4H-naphthalen-1-one

C12H12O3

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)n2c(C3(O)C=CC(=O)c4ccccc43)cc3ccccc32)cc1
HCID10387927

未命名化合物

收率 23%

PROCEDURE

实验过程

The title compound was prepared from 4,4-dimethoxy-4H-naphthalen-1-one and 1-(toluene4-sulfonyl)-1H-indole, according to Method E, described above. Yield 23%; mp 110-112° C.; 1H NMR (CDCl3) δ 8.35-8.39 (dd, J=8 Hz, 1H), 8.04 (d, J=8 Hz,1H), 7.74-7.97 (m, 6H), 7.32-7.48 (m, 6H), 6.53 (d, J=10 Hz,1H), 2.52 (s, 3H); 13C NMR (CDCl3) δ 189.7, 154.0, 150.2, 149.8, 148.8, 143.6, 140.1, 137.9, 135.7, 134.8, 133.6, 132.3, 131.7, 131.3, 130.7, 129.3, 126.6, 120.4, 120.3, 74.8, 26.6; MS (AP+) m/z 430.09 (M++1), 412.14.