2-羟基-3-甲氧基苄醇 → [3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

HRID 1176464

反应方程式

HRID 1176464 反应方程式
[OH:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([O:9][CH3:10])[C:4]=1[OH:11].[CH3:12][O:13][CH2:14][CH2:15]Br>>[CH3:10][O:9][C:5]1[C:4]([O:11][CH2:15][CH2:14][O:13][CH3:12])=[C:3]([CH2:2][OH:1])[CH:8]=[CH:7][CH:6]=1

参与物

3

反应物 2

HCID 780882-羟基-3-甲氧基苄醇HCID 809722-溴乙基甲基醚

产物 1

HCID 43471496[3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

实验过程

Analogously to Method F, 2.44 g of 2-hydroxymethyl-6-methoxyphenol and 2.56 g of 2-bromoethyl methyl ether are reacted and the title compound is obtained as a colourless oil. Rf=0.22 (1:1 EtOAc-heptane); Rt=2.91.

来源与证据

ORD记录
ord-fc59f8e97f4a491a90816f2b711a523b
来源数据集
uspto-grants-2010_11
专利号
US07842688B2

关联笔记

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