2-羟基-3-甲氧基苄醇 → [3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

HRID 1176466

反应方程式

HRID 1176466 反应方程式
[OH:1][CH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([O:9][CH3:10])[C:4]=1[OH:11].ClC[CH2:14][CH2:15][O:16][CH3:17]>>[CH3:10][O:9][C:5]1[C:4]([O:11][CH2:14][CH2:15][O:16][CH3:17])=[C:3]([CH2:2][OH:1])[CH:8]=[CH:7][CH:6]=1

参与物

3

反应物 2

HCID 780882-羟基-3-甲氧基苄醇HCID 1189273-氯丙基甲基醚

产物 1

HCID 43471496[3-Methoxy-2-(2-methoxyethoxy)phenyl]methanol

实验过程

Analogously to Method F, 2.67 g of 2-hydroxymethyl-6-methoxyphenol and 2.19 g of 1-chloro-3-methoxypropane are reacted. The title compound is obtained as a colourless oil. Rf=0.23 (1:1 EtOAc-heptane); Rt=3.08.

来源与证据

ORD记录
ord-0e1389e3b17549d1ac151a08daaf8ec4
来源数据集
uspto-grants-2010_11
专利号
US07842688B2

关联笔记

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