肼(无水) → 2-肼基-4,8-二甲基喹啉

HRID 1892271

反应方程式

HRID 1892271 反应方程式
Cl[C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1.[NH2:14][NH2:15]>>[NH:14]([C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1)[NH2:15]

参与物

3

实验过程

A solution of 2-chloro-4,8-dimethylquinoline (1.00 g, 5.2 mmoles) in NH2NH2 was reacted as outlined in Scheme 1 above to give the desired title compound which was used in the next step without further purification.

来源与证据

ORD记录
ord-6e7151b8bb97483b9a7a27f298eca9e7
来源数据集
uspto-grants-2013_08
专利号
US08507682B2

关联笔记

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