多聚甲醛 → Formaldehyde melamine silicate melamine

HRID 258532

反应方程式

HRID 258532 反应方程式
O[Si](O)=O.[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7].[CH2:14]=[O:15].S(=O)(=O)(O)O.[Si:21]([OH:25])([OH:24])([OH:23])[OH:22]>>[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7].[Si:21]([OH:25])([OH:24])([OH:23])[OH:22].[N:5]1[C:12]([NH2:13])=[N:11][C:9]([NH2:10])=[N:8][C:6]=1[NH2:7].[CH2:14]=[O:15]

参与物

6

反应物 5

HCID 712多聚甲醛HCID 1118四氧化硫HCID 7955三聚氰胺2 次HCID 14768硅酸HCID 14942原硅酸

产物 1

HCID 131710832Formaldehyde melamine silicate melamine

实验过程

The mixture of polysiliconformic acid, orthosilicoformic acid, silicoformic acid and metasilicic acid as produced in Example XIV are mixed with 30 parts by weight of melamine and added to 100 parts by weight of an aqueous solution containing about 37% formaldehyde, then dilute sulfuric acid is added until the pH is 4 to 6. The mixture is heated to 70° to 100° C., while agitating; the silicic acid and melamine go into solution, and, in 20 to 60 minutes or until the desired viscosity is obtained, produces a white poly (formaldehyde melamine silicate melamine silicoformate) resin. The said resin softens with heat and may be molded into useful objects. The said resin is soluble in acetic acid and, when applied to wood and dried, it produces a tough clear protective coating.

后处理

  1. customas produced in Example XIV
  2. additionadded to 100 parts by weight of an aqueous solution
  3. temperatureThe mixture is heated to 70° to 100° C.
  4. customuntil the desired viscosity is obtained

来源与证据

ORD记录
ord-cf9fd26add1b4205882bdf954c50550f
来源数据集
uspto-grants-1977_07
专利号
US04033935

关联笔记

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