碘甲烷 → HCID 20515175，化合物

HRID 26549

反应方程式

HRID 26549 反应方程式
[NH2:1][C:2]1[CH:3]=[C:4]([C:14](=[O:20])[C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:5]=[CH:6][C:7]=1[CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1.[CH3:21]I>N1C=CC=CC=1>[CH3:21][NH:1][C:2]1[CH:3]=[C:4]([C:14](=[O:20])[C:15]([O:17][CH2:18][CH3:19])=[O:16])[CH:5]=[CH:6][C:7]=1[CH:8]1[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1

参与物

4

反应物 2

HCID 6328碘甲烷HCID 20515218Ethyl 3-amino-4-cyclohexylphenylglyoxylate

产物 1

HCID 20515175HCID 20515175，化合物

试剂、催化剂与溶剂 1

HCID 1049吡啶溶剂

实验过程

To a solution of 0.01 moles of ethyl 3-amino-4-cyclohexylphenylglyoxylate in 100 ml. of pyridine is added 0.1 moles of methyl iodide. The reaction mixture is stirred overnight at room temperature, filtered and concentrated. The residue is distilled to obtain ethyl 3-methylamino-4-cyclohexylphenylglyoxylate.

后处理

  1. filtrationfiltered
  2. concentrationconcentrated
  3. distillationThe residue is distilled

来源与证据

ORD记录
ord-a2e369448a4f40eea2bd19b445797bbb
来源数据集
uspto-grants-1979_04
专利号
US04150148

关联笔记

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