天然气 → Hydroquinone methane

HRID 2661

反应方程式

HRID 2661 反应方程式
[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].[CH4:9]>C(O)CC>[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].[CH4:9]

参与物

4

反应物 2

HCID 297天然气HCID 785对苯二酚

产物 1

HCID 18985114Hydroquinone methane

试剂、催化剂与溶剂 1

HCID 1031正丙醇溶剂

实验过程

Hydroquinone (30 g) was dissolved in n-propanol (70 ml) at 70° C. The hot solution was introduced into the high pressure autoclave. The solution was subjected to compressed methane of 300 bar. The high pressure autoclave was kept for 2 h at 80° C. The solution was then cooled down to room temperature within 5 days. The crystals were filtered off and then washed 4 times with cold n-propanol (5 ml). The crystals were dried in the drying cabinet at 70° C. subsequently.

后处理

  1. additionThe hot solution was introduced into the high pressure autoclave
  2. filtrationThe crystals were filtered off
  3. washwashed 4 times with cold n-propanol (5 ml)
  4. customThe crystals were dried in the drying cabinet at 70° C. subsequently

来源与证据

ORD记录
ord-4ada581c5e0b46f1931dbf7d4b1bd141
来源数据集
uspto-grants-1998_03
专利号
US05730954

关联笔记

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