丁醇 → HCID 178514811，化合物

HRID 324144

反应方程式

HRID 324144 反应方程式
[Ir:1].[Ta:2].C([OH:7])CCC>[Ti]>[Ir:1]=[O:7].[O-2:7].[Ta+5:2].[O-2:7].[O-2:7].[O-2:7].[O-2:7].[Ta+5:2]

参与物

5

反应物 3

HCID 263丁醇HCID 23924铱2 次HCID 23956氢化钽2 次

产物 1

HCID 178514811HCID 178514811，化合物

试剂、催化剂与溶剂 1

HCID 23963Titanium催化剂

实验过程

After the roughened titanium substrate surface was heat treated, it was painted with a n-butanol solution containing salts of iridium and tantalum. The ratio of iridium to tantalum in the solution was about 65% to 35% by weight. The solution was allowed to dry at ambient temperature for approximately 20 minutes. The painted titanium substrate was subsequently heat treated in a furnace having an oxygen containing atmosphere at approximately 500° C. for approximately 20-30 minutes to form an iridium oxide/tantalum oxide composite coating. The process of painting and heat treating the titanium substrate was repeated to obtain a first layer having a total loading of 2.0 g/m2. After the desired loading was achieved, the anode was heat treated for approximately one hour at approximately 500° C.

后处理

  1. additiontreated
  2. customto dry at ambient temperature for approximately 20 minutes
  3. temperatureThe painted titanium substrate was subsequently heat
  4. additiontreated in a furnace
  5. customat approximately 500° C.
  6. customfor approximately 20-30 minutes

来源与证据

ORD记录
ord-c7848c10c67f4658b8f52f05a07d6b97
来源数据集
uspto-grants-2001_04
专利号
US06217729B1

关联笔记

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