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吡啶 → 9-Anthracenylmethyl-1-piperazinecarboxylate
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 吡啶 | HCID 1049 | — |
| 反应物 | 哌嗪 | HCID 4837 | — |
| 反应物 | 9-蒽醇 | HCID 73848 | — |
| 反应物 | 对硝基苯基氯甲酸酯 | HCID 82129 | — |
| 溶剂 | 聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯] | HCID 962 | — |
| 产物 | 9-Anthracenylmethyl-1-piperazinecarboxylate | HCID 9840073 | — |
反应步骤
PAC is produced by adding 9-anthacenemethanol and pyridine to a solution of p-nitrophenyl chloroformate. Product is isolated to provide a crude anthrylmethyl p-nitrophenyl carbonate, which is then added to a solution of piperazine. The reacted mixture is poured into water and extracted with a solvent, preferably an organic solvent such as toluene. The product is washed and dried to provide 9-anthracenylmethyl-1-piperazinecarboxylate (PAC).
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US06656737B1 |
| 来源数据集 | uspto-grants-2003_12 |
| ORD ID | ord-93be286c94a04903a525ad5c7e904ac7 |
| 来源说明 | uspto-grants-2003_12 |