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HRID 43294生成日期:2026年10月23日

四氢噻吩 → Methyl-tetrahydrothiophene triflate

https://huagongshe.com/zh-CN/reaction/43294

反应方程式

参与物

角色名称HCID投料
反应物四氢噻吩HCID 1127—
反应物三氟甲烷磺酸甲酯HCID 9526—
溶剂二氯甲烷HCID 6344—
产物Methyl-tetrahydrothiophene triflateHCID 87659244—

反应步骤

11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

来源与证据

DOI10.6084/m9.figshare.5104873.v1
专利号US08536347B2
来源数据集uspto-grants-2013_09
ORD IDord-9dffcd1064074e23ac42b75b8afab9eb
来源说明uspto-grants-2013_09