化工社化工社化学信息打印报告 · 仅供科研参考
四氢噻吩 → Methyl-tetrahydrothiophene triflate
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 四氢噻吩 | HCID 1127 | — |
| 反应物 | 三氟甲烷磺酸甲酯 | HCID 9526 | — |
| 溶剂 | 二氯甲烷 | HCID 6344 | — |
| 产物 | Methyl-tetrahydrothiophene triflate | HCID 87659244 | — |
反应步骤
11 mmol of tetrahydrothiophene was dissolved in 10 ml of dichloromethane at 0° C., and about 12 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. As a result, a white solid product in a salt form was obtained after about 5 minutes. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US08536347B2 |
| 来源数据集 | uspto-grants-2013_09 |
| ORD ID | ord-9dffcd1064074e23ac42b75b8afab9eb |
| 来源说明 | uspto-grants-2013_09 |