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2-苯基-1-丙醇 → N-[4-(2-Phenylpropoxy)benzoyl]glycine
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 2-苯基-1-丙醇 | HCID 14295 | — |
| 反应物 | N-(4-Hydroxybenzoyl)glycine tert-butyl ester | HCID 10682169 | — |
| 产物 | N-[4-(2-Phenylpropoxy)benzoyl]glycine | HCID 66812487 | 72% |
反应步骤
The same reaction as in Example 1 (1b) was conducted using N-(4-hydroxybenzoyl)glycine tert-butyl ester (247 mg, 0.983 mmol) prepared in Example 1 (1a) and 2-phenylpropan-1-ol (185 μL, 1.32 mmol) to give 221 mg of the title compound (white powder, yield: 72%).
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US08497397B2 |
| 来源数据集 | uspto-grants-2013_07 |
| ORD ID | ord-732fcd1126af40698b572ccf3ab0506e |
| 来源说明 | uspto-grants-2013_07 |