丙二酸钠 → Zinc Malonate Dihydrate

HRID 733500

反应方程式

HRID 733500 反应方程式
O.O.N[C@H](C([O-])=O)CCC([O-])=[O:8].[Zn+2:13].C([O-])(=O)CC([O-])=[O:17].[Na+].[Na+].[CH2:23]([C:27]([O-:29])=[O:28])[C:24]([O-:26])=[O:25].[Cl-].[Zn+2].[Cl-]>O>[OH2:8].[OH2:17].[C:27]([O-:29])(=[O:28])[CH2:23][C:24]([O-:26])=[O:25].[Zn+2:13]

参与物

6

反应物 4

HCID 8865丙二酸钠HCID 9084丙二酸HCID 3007855氯化锌HCID 22825209Zinc L-glutamate Dihydrate

产物 1

HCID 86616729Zinc Malonate Dihydrate

试剂、催化剂与溶剂 1

HCID 962聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯]溶剂

实验过程

Basically the reaction conditions found for preparation of zinc L-glutamate (Example 13) was employed. A suspension of sodium malonate (white coloured) is prepared by adding 100 mL of millipore water to 16.605 g (0.1 moles) of solid sodium malonate dibasic monohydrate (SIGMA M1875-100G, MW 166.05, CAS 26522-85-0) in a 250 mL beaker. To this suspension was added 13.628 g (0.1 moles) of solid zinc chloride (FLUKA, 96469, MW 136.3, CAS 7646-85-7). Subsequent manufacturing steps were as described in Example 13.

后处理

  1. customBasically the reaction conditions
  2. customis prepared

来源与证据

ORD记录
ord-61926276b95f4951b769df7926e9ab35
来源数据集
uspto-grants-2009_09
专利号
US07589235B2

关联笔记

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