Hydrogen Peroxide → 二异丁酰基过氧化物

HRID 8140

反应方程式

HRID 8140 反应方程式
[OH:1][OH:2].[C:3](Cl)(=[O:7])[CH:4]([CH3:6])[CH3:5]>O>[C:3]([O:1][O:2][C:3](=[O:7])[CH:4]([CH3:6])[CH3:5])(=[O:7])[CH:4]([CH3:6])[CH3:5]

参与物

4

反应物 2

HCID 784Hydrogen PeroxideHCID 62325异丁酰氯

产物 1

HCID 76969二异丁酰基过氧化物

试剂、催化剂与溶剂 1

HCID 962聚[6-[4-(4-氰基苯基)苯氧基]己基甲基丙烯酸酯]溶剂2 次

实验过程

In Example A, the procedure of WO 01/32613 was repeated. First, a solution of Na2O2 was prepared by combining 108.3 g of demineralized water, 18.5 g of NaOH-33 solution, and 3.7 g of the aqueous H2O2. A second reactor was charged with 33.3 g of demineralized water, 27.7 g of the PVA solution, and 16.3 g of isobutanoyl chloride while controlling the temperature between 5–10° C. Next, the Na2O2 solution was dosed while the system was homogenized. No diisobutanoyl peroxide was obtained and only an aqueous phase formed.

后处理

  1. customFirst, a solution of Na2O2 was prepared
  2. custombetween 5–10° C

来源与证据

ORD记录
ord-9ab80e1ebfc347c382d0c4a31e189f35
来源数据集
uspto-grants-2006_08
专利号
US07087693B2

关联笔记

加载中…