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溴化苄 → 6-(5-Ethyl-1,3,4-thiadiazol-2-ylthiomethyl)-4-morpholino-2-[6-(2-propenyloxycarbonylamino)-2-pyridylmethylamino]pyridine
参与物
| 角色 | 名称 | HCID | 投料 |
|---|---|---|---|
| 反应物 | 溴化苄 | HCID 7498 | — |
| 反应物 | 6-氯甲基吡啶-3-甲酸乙酯 | HCID 15614003 | — |
| 反应物 | (+/-)-6-[1-(5-Ethyl-1,3,4-thiadiazol-2-ylthio)ethyl]-4-morpholino-2-[3-(2-propenyloxycarbonylamino)benzylamino]pyridine | HCID 19369555 | — |
| 产物 | 6-(5-Ethyl-1,3,4-thiadiazol-2-ylthiomethyl)-4-morpholino-2-[6-(2-propenyloxycarbonylamino)-2-pyridylmethylamino]pyridine | HCID 19369722 | — |
反应步骤
The above identified compound was obtained as a pale yellow solid in the same manner as in Example 1-(6), Example 4-(2) and (3) and Example 1-(7) except that benzyl bromide was changed to ethyl 6-chloromethylpyridine-2-carboxylate.
来源与证据
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 专利号 | US06011039 |
| 来源数据集 | uspto-grants-2000_01 |
| ORD ID | ord-882efe6d3d154f0697354f081212610a |
| 来源说明 | uspto-grants-2000_01 |