Acetyl chloride → N-Methyl-phenylglycine methyl ester hydrochloride

Beteiligte Stoffe

Reaktionsschritte

Prepared by Method A of Example 19 but using N-methyl-phenylglycine (prepared in turn from 2-chlorophenylacetic acid and methylamine) (3.5 g) methanol (20 ml) and acetyl chloride (40 ml) over 48 hours. The title compound was obtained in 94% yield, after trituration with methanol, as a white solid.

Herkunft & Nachweise