HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Acetic Acid → Ethyl 2-(9-xanthyl)-3-oxo-3-[3-(phenacylmethyloxycarbonyl)cyclobutyl]propanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Acetic Acid | HCID 176 | — |
| Edukt | Xanthydrol | HCID 72861 | — |
| Edukt | Ethyl 3-oxo-3-[3-(phenacylmethyloxycarbonyl) cyclobutyl]propanate | HCID 18791135 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | Ethyl 2-(9-xanthyl)-3-oxo-3-[3-(phenacylmethyloxycarbonyl)cyclobutyl]propanate | HCID 18791133 | — |
Reaktionsschritte
Acetic acid (20 ml) was added to a stirred suspension of 9-hydroxyxanthene (3.96 g, 20 mmol) and ethyl 3-oxo-3-[3-(phenacylmethyloxycarbonyl) cyclobutyl]propanate (6.0 g, 18 mmol) in ethanol (20 ml) at room temperature. A clear solution formed and was allowed to stand for 7 days at room temperature.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06054448 |
| Quelldatensatz | uspto-grants-2000_04 |
| ORD ID | ord-d2a13ead311f457bbe212e4d69a20f70 |
| Quellennotiz | uspto-grants-2000_04 |