HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1,1-Dibutoxycyclohexane → 2-(1-Butoxycyclohexyloxy)methyl-5-(3,5-dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazole
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1,1-Dibutoxycyclohexane | HCID 243718 | — |
| Edukt | (5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol | HCID 473933 | — |
| Produkt | 2-(1-Butoxycyclohexyloxy)methyl-5-(3,5-dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazole | HCID 18792052 | 35% |
Reaktionsschritte
The compound 19 (345 mg, 1.00 mmol) was converted to the acetal with 1,1-dibutoxycyclohexane (2.28 g, 10.0 mmol) in the same manner as the example 18 to give the compound 21 (172 mg, 35%) as oil. Rf 0.41 (Al2O3 60, Type E, toluene).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06054591 |
| Quelldatensatz | uspto-grants-2000_04 |
| ORD ID | ord-b97b14f4d45547458ad5b9ca3ec6d6e1 |
| Quellennotiz | uspto-grants-2000_04 |