Hydrochloric Acid → Ethyl 2-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}acetate

HRID 1008106

Reaktionsgleichung

Reaktionsgleichung von HRID 1008106
[C:1]([C:3]1[CH:8]=[CH:7][C:6]([S:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])=[CH:5][CH:4]=1)#[N:2].[Al](Br)(Br)Br.[Cl:20][C:21]([Cl:25])([Cl:24])[C:22]#[N:23].[ClH:26]>>[Cl:20][C:21]([Cl:25])([Cl:24])[C:22]1[N:23]=[C:22]([C:21]([Cl:24])([Cl:20])[Cl:26])[N:23]=[C:1]([C:3]2[CH:4]=[CH:5][C:6]([S:9][CH2:10][C:11]([O:13][CH2:14][CH3:15])=[O:12])=[CH:7][CH:8]=2)[N:2]=1

Komponenten

5

Edukt 4

HCID 313Hydrochloric AcidHCID 11011TrichloroacetonitrileHCID 24409Aluminum bromideHCID 22666606Ethyl 2-(4-cyanophenyl thio)acetate

Produkt 1

HCID 86759533Ethyl 2-{4-[2,4-bis(trichloromethyl)-s-triazine-6-yl]phenyl thio}acetate

Versuchsvorschrift

The mixed solution of 10 g of ethyl 2-(4-cyanophenyl thio)acetate (45.2 mmol), 0.8 g of AlBr3, and 50 g of trichloroacetonitrile were bubbled with dry HCl at room temperature.

Quellen und Nachweise

ORD-Eintrag
ord-38b8d5030c93492ab327dd87e993ee8d
Quelldatensatz
uspto-grants-2004_09
Patentnummer
US06797739B1

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