HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Azobisisobutyronitrile → Butyl Acrylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Azobisisobutyronitrile | HCID 6547 | — |
| Edukt | Butyl Acrylate | HCID 8846 | — |
| Edukt | 2-Hydroxyethyl acrylate | HCID 13165 | — |
| Edukt | Stearyl acrylate | HCID 62552 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | Butyl Acrylate | HCID 8846 | — |
| Produkt | Stearyl acrylate | HCID 62552 | — |
| Produkt | HCID 178473601 | HCID 178473601 | — |
Reaktionsschritte
To a 1 L flask equipped with a stirrer, a nitrogen introducing tube, a thermometer and a condenser, 50 g of stearyl acrylate, 49 g of n-butylacrylate, 1 g of hydroxyethyl acrylate, 0.89 g of AIBN, 100 mL of toluene and 100 mL of ethyl acetate were added and subjected to polymerization reaction in a stream of nitrogen at 70° C. for 12 hr, to obtain a copolymer of stearyl acrylate, n-butyl acrylate and hydroxyacrylate (hereinafter sometimes referred to “PSABAHEA”. The resulting PSABAHEA had a weight average molecular weight of 170,000.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07976921B2 |
| Quelldatensatz | uspto-grants-2011_07 |
| ORD ID | ord-8bc452f0ce8242eeb56d756833558e2b |
| Quellennotiz | uspto-grants-2011_07 |