Hydrochloric Acid → HCID 54402950, Verbindung

HRID 1010522Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1010522
C([O:3][C:4](=[O:13])[CH2:5][N:6]1[CH:10]=[C:9]([CH2:11][CH3:12])[N:8]=[CH:7]1)C.Cl>>[CH2:11]([C:9]1[N:8]=[CH:7][N:6]([CH2:5][C:4]([OH:13])=[O:3])[CH:10]=1)[CH3:12]

Komponenten

3

Edukt 2

HCID 313Hydrochloric AcidHCID 57731307HCID 57731307, Verbindung

Produkt 1

HCID 54402950HCID 54402950, Verbindung

Versuchsvorschrift

1.7 g (9.5 mmol) of (4-ethyl-imidazol-1-yl)-acetic acid ethyl ester are dissolved in 47 ml (190 mmol) 4N HCl and the mixture is heated to reflux. After 2 h the mixture is cooled to rt and the solvent is removed in vacuo. The resulting product is used without further purification.

Aufarbeitung

  1. temperaturethe mixture is heated to reflux
  2. customthe solvent is removed in vacuo
  3. customThe resulting product is used without further purification

Quellen und Nachweise

ORD-Eintrag
ord-bb57c63f9b0d41b99bff4471bff17847
Quelldatensatz
uspto-grants-2011_07
Patentnummer
US07977323B2

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